What is the CAS number of PdCl2 DPPF )- ch2cl2adduct?

Synthesis Process

The synthesis of 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex involves a straightforward procedure:

1. Dissolve 2.00 grams of sodium palladium chloride in 30mL of anhydrous ethanol to get the ethanol solution of sodium palladium chloride.
2. Dissolve 4.15 grams of 1,1'-bis(diphenylphosphine)ferrocene in 41mL dichloromethane to obtain 1,1'-bis(diphenylphosphine)ferrocene dichloromethane solution.
3. Under stirring conditions, add the ethanol solution of sodium palladium chloride from step 1 to the dichloromethane solution from step 2, and stir for 1 hour at 25°C. The resulting complex crystal is achieved with a yield of 90.46%.

This synthesis method efficiently utilizes dichloromethane as a solvent in a single-step process, thereby simplifying the procedure and shortening the synthesis cycle. The produced complex has a purity level of 99.4%.

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Safety Recommendations

Regarding safety, the following measures should be strictly adhered to:

• Keep the container in a well-ventilated place.
• Wear suitable protective clothing and gloves.
• This material and its container must be disposed of as hazardous waste.